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Experimental (top) and simulated (bottom) 51V solid-state NMR spectra of [VO(hshed)(Cat)] acquired at the MAS frequencies of (a) 7 kHz, (b) 13 kHz, (c) 17 kHz and (d) 20 kHz. The spectra were simulated with the following parameters: CQ = 4.0 ± 0.1 MHz; δσ= −243 ± 30 ppm; ηQ = 1.0 ± 0.05; ησ = 0.93 ± 0.05; α = 81 ± 10; β= 70 ± 15; γ = 87 ± 15.
