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. 2012 Jun 28;68(Pt 7):824–828. doi: 10.1107/S1744309112019082

Table 1. Crystal data and data-collection statistics.

Values in parentheses are for the outermost shell.

X-ray source ID23-2
Wavelength (Å) 0.873
No. of images 40
Oscillation range (°) 1.0
Unit-cell parameters (Å) a = b = 116.12, c = 158.93
Space group P42212
No. of molecules in asymmetric unit 2
Matthews coefficient (Å3 Da−1) 2.76
Solvent content (%) 55.5
Resolution range (Å) 45–3.0
Unique reflections 22073 (3143)
Observed reflections [I/σ(I) > 1] 72116 (10301)
Completeness (%) 99.0 (98.4)
R merge 16.6 (56.6)
Mean I/σ(I) 8.5 (3.1)

R merge = Inline graphic Inline graphic calculated for the whole data set.