Table 1. Crystal data and data-collection statistics.
Values in parentheses are for the outermost shell.
| X-ray source | ID23-2 |
| Wavelength (Å) | 0.873 |
| No. of images | 40 |
| Oscillation range (°) | 1.0 |
| Unit-cell parameters (Å) | a = b = 116.12, c = 158.93 |
| Space group | P42212 |
| No. of molecules in asymmetric unit | 2 |
| Matthews coefficient (Å3 Da−1) | 2.76 |
| Solvent content (%) | 55.5 |
| Resolution range (Å) | 45–3.0 |
| Unique reflections | 22073 (3143) |
| Observed reflections [I/σ(I) > 1] | 72116 (10301) |
| Completeness (%) | 99.0 (98.4) |
| R merge † | 16.6 (56.6) |
| Mean I/σ(I) | 8.5 (3.1) |
R
merge =
calculated for the whole data set.