Table 1. Data-collection and processing statistics for TgISP1-2.
Crystal form 1 | Crystal form 2 | |
---|---|---|
Space group | P4132 or P4332 | P212121 |
Unit-cell parameters (Å, °) | a = b = c = 129.21, α = β = γ = 90 | a = 58.11, b = 81.09, c = 120.07, α = β = γ = 90 |
Wavelength | 0.9795 | 1.54 |
Resolution range (Å) | 43.07–2.05 (2.16–2.05) | 29.09–2.10 (2.21–2.10) |
Measured reflections | 362703 | 160946 |
Unique reflections | 23759 | 33884 |
Multiplicity | 15.3 (13.3) | 4.7 (4.8) |
Completeness (%) | 100.0 (100.0) | 99.9 (100.0) |
〈I/σ(I)〉 | 15.1 (4.8) | 16.3 (4.5) |
R merge † | 0.102 (0.469) | 0.069 (0.380) |
R merge = , where 〈I(hkl)〉 is the average of symmetry-related observations of a unique reflection.