Bruker APEXII CCD diffractometer | 1983 independent reflections |
Radiation source: fine-focus sealed tube | 1558 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.055 |
φ and ω scans | θmax = 25.3°, θmin = 2.9° |
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −13→12 |
Tmin = 0.938, Tmax = 0.989 | k = −11→11 |
5135 measured reflections | l = −17→25 |