Table 1.
Data collection and refinement statistics (molecular replacement)
| Parameter | Value for BNPb |
|---|---|
| Data collection statistics | |
| Space group | I 2 2 2 |
| Cell dimensions | |
| a, b, c (Å) | 106.95, 123.34, 198.08 |
| α, β, γ (°) | 90.00, 90.00, 90.00 |
| Resolution (Å) | 104.73–3.23 (3.35–3.23)a |
| Rsym or Rmerge | 0.113 (0.387) |
| I /σI | 13.8 (2.9) |
| Completeness (%) | 93.2 (95.1) |
| Redundancy | 7.2 (7.3) |
| Refinement statistics | |
| Resolution range (Å) | 47.055–3.233 |
| No. of reflections | 19,862 |
| Rwork/Rfree | 0.245/0.291 |
| No. of atoms | 7022 |
| B-factors | 77.10 |
| RMSD | |
| Bond lengths (Å) | 0.002 |
| Bond angles (°) | 0.729 |
| Ramachandran plot (%) | |
| Most favored | 88.5 |
| Additional allowed | 9.0 |
| Generously allowed | 2.5 |
| Disallowed | 0.0 |
a
Data from a single crystal.
b
Values in parentheses are for highest-resolution shell.