| Bruker APEXII CCD area-detector diffractometer | 2103 reflections with I > 2σ(I) |
| ω scans | Rint = 0.037 |
| Absorption correction: integration (XPREP; Bruker, 2004) | θmax = 28°, θmin = 2.2° |
| Tmin = 0.332, Tmax = 0.746 | h = −37→40 |
| 11693 measured reflections | k = −12→11 |
| 2705 independent reflections | l = −9→9 |