| Bruker SMART CCD area-detector diffractometer | 2456 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.067 |
| Graphite monochromator | θmax = 27.5°, θmin = 2.2° |
| phi and ω scans | h = −12→13 |
| 18815 measured reflections | k = −19→19 |
| 3763 independent reflections | l = −15→15 |
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