| Agilent SuperNova Dual diffractometer with an Atlas detector | 1542 independent reflections |
| Radiation source: SuperNova (Cu) X-ray Source | 1169 reflections with I > 2σ(I) |
| Mirror monochromator | Rint = 0.018 |
| Detector resolution: 10.4041 pixels mm-1 | θmax = 76.0°, θmin = 3.2° |
| ω scan | h = −16→17 |
| Absorption correction: multi-scan (CrysAlis PRO; Agilent, 2012) | k = −3→4 |
| Tmin = 0.476, Tmax = 1.000 | l = −17→17 |
| 2474 measured reflections |
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