| Rigaku R-AXIS RAPID diffractometer | 1552 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.030 |
| Graphite monochromator | θmax = 25.0°, θmin = 2.8° |
| ω scans | h = −17→17 |
| 9046 measured reflections | k = −7→7 |
| 2265 independent reflections | l = −16→17 |
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