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. 2012 Jun 7;10(6):1297–1306. doi: 10.3390/md10061297

Table 2.

NMR spectroscopic data forauranomide C (3) in DMSO-d6.

Position δH (J in Hz) HMBC a
2 155.8, C
4 161.0, C
5 121.0, C
6 126.8, CH 8.19, dd (8.0, 1.0) 4, 8, 10
7 128.8, CH 7.60, t (8.0) 5, 9
8 135.2, CH 7.91, td (8.0, 1.0) 6, 10
9 127.4, CH 7.76, d (8.0) 5, 7
10 145.9, C
11 53.2, CH 4.16, m 2, 12, 13
12 24.1, CH2 2.15, 2.34, m 2, 11, 13, 14
13 30.8, CH2 2.29, m 11, 12, 14
14 173.7, C
15 N-H, 6.76, brs 13, 14
N-H, 7.26, brs 14
16 N-H, 8.82, d, (7.0) 11, 12, 18
17 130.7, C
18 131.2, C
19 128.9, CH 7.78, dd (8.5, 1.5) 17, 21, 23
20 127.6, CH 7.59, td (8.5, 1.5) 18, 22
21 128.6, CH 7.67, td (8.5, 1.5) 17, 19
22 133.0, CH 7.64, dd (8.5, 1.5) 18, 20
23 166.9, C

a HMBC correlations, optimized for 8 Hz, are from proton(s) stated to the indicated carbon.