Table 2.
Position | δH (J in Hz) | HMBC a | |
---|---|---|---|
2 | 155.8, C | ||
4 | 161.0, C | ||
5 | 121.0, C | ||
6 | 126.8, CH | 8.19, dd (8.0, 1.0) | 4, 8, 10 |
7 | 128.8, CH | 7.60, t (8.0) | 5, 9 |
8 | 135.2, CH | 7.91, td (8.0, 1.0) | 6, 10 |
9 | 127.4, CH | 7.76, d (8.0) | 5, 7 |
10 | 145.9, C | ||
11 | 53.2, CH | 4.16, m | 2, 12, 13 |
12 | 24.1, CH2 | 2.15, 2.34, m | 2, 11, 13, 14 |
13 | 30.8, CH2 | 2.29, m | 11, 12, 14 |
14 | 173.7, C | ||
15 | N-H, 6.76, brs | 13, 14 | |
N-H, 7.26, brs | 14 | ||
16 | N-H, 8.82, d, (7.0) | 11, 12, 18 | |
17 | 130.7, C | ||
18 | 131.2, C | ||
19 | 128.9, CH | 7.78, dd (8.5, 1.5) | 17, 21, 23 |
20 | 127.6, CH | 7.59, td (8.5, 1.5) | 18, 22 |
21 | 128.6, CH | 7.67, td (8.5, 1.5) | 17, 19 |
22 | 133.0, CH | 7.64, dd (8.5, 1.5) | 18, 20 |
23 | 166.9, C |
a HMBC correlations, optimized for 8 Hz, are from proton(s) stated to the indicated carbon.