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. 2012 Apr 27;10(5):987–997. doi: 10.3390/md10050987

Table 1.

1H and 13C NMR data for 1 and 2.

Position 1 2
δH (J in Hz) a δC (mult.) b δH (J in Hz) a δC (mult.) b
1 1.46 m; 0.98 m 40.2 (CH2) c 1.65 m 39.9 (CH2)
2 1.65 m; 1.40 m 18.4 (CH2) 1.54 m; 1.38 m 18.2 (CH2)
3 1.38 m; 1.19 m 42.5 (CH2) 1.36 m; 1.12 m 42.0 (CH2)
4 33.1 (C) 33.3 (C)
5 0.92 m 57.6 (CH) 0.80 m 56.5 (CH)
6 1.57 m; 1.38 m 18.8 (CH2) 1.61 m; 1.42 m 18.6 (CH2)
7 1.68 m; 1.10 m 40.1 (CH2) 1.74 m; 0.90 m 41.7 (CH2)
8 44.8 (C) 37.3 (C)
9 1.45 m 61.0 (CH) 0.88 m 58.9 (CH)
10 36.8 (C) 37.5 (C)
11 1.99 d (6.0); 1.43 m 35.0 (CH2) 1.70 m; 1.45 m 27.5 (CH2)
12 43.0 (C) 3.40 br d (10.5) 80.5 (CH)
13 2.20 dd (13.0, 2.5) 47.5 (CH) 42.0 (C)
14 2.64 dd (13.5, 13.0) 39.6 (CH2) 0.80 m 58.1(CH)
2.54 dd (13.5, 2.5)
15 196.8 (C) 1.78 m; 1.36 m 20.0 (CH2)
16 122.9 (C) 2.20 m; 1.22 m 25.6 (CH2)
17 159.0 (C) 2.22 m 39.2 (CH)
18 4.58 s 75.9 (CH) 1.86 m 55.3 (CH)
19 0.85 s 33.5 (CH3) 0.84 s 33.2 (CH3)
20 0.84 s 21.3 (CH3) 0.80 s 21.3 (CH3)
21 0.85 s 16.2 (CH3) 0.84 s 17.3 (CH3)
22 0.87 s 15.6 (CH3) 0.84 s 16.3 (CH3)
23 1.14 s 23.4 (CH3) 0.91 s 9.8 (CH3)
24 7.33 d (1.5) 142.3 (CH) 177.8 (C)
25 6.76 d (1.5) 110.9 (CH) 4.38 dd (9.5, 7.0) 70.0 (CH2)
      4.09 dd (11.0, 10.0)  

a 500 MHz in CDCl3; b 125 MHz in CDCl3; c Numbers of attached protons were deduced by DEPT experiments.