1 |
isopropanol/acetic acid (v/v,4:1) |
20 |
100 |
100 |
100 |
59.0 |
2 |
acetonitrile/acetic acid (v/v, 4:1) |
20 |
100 |
100 |
100 |
40.1 |
3 |
chloroform/acetic acid (v/v, 4:1) |
20 |
100 |
100 |
100 |
43.9 |
4 |
isopropanol/acetic acid (v/v, 4:2) |
20 |
100 |
100 |
100 |
51.3 |
5 |
isopropanol/acetic acid (v/v, 4:1) |
10 |
100 |
100 |
100 |
45.1 |
6 |
isopropanol/acetic acid (v/v, 4:1) |
30 |
100 |
100 |
100 |
62.5 |
7 |
isopropanol/acetic acid (v/v, 4:1) |
20 |
130 |
100 |
130 |
69.6 |
8 |
isopropanol/acetic acid (v/v, 4:1) |
20 |
150 |
100 |
150 |
79.0 |
9 |
isopropanol/acetic acid (v/v, 4:1) |
20 |
170 |
100 |
170 |
77.0 |
10 |
isopropanol/acetic acid (v/v, 4:1) |
20 |
150 |
60 |
100 |
43.0 |
11 |
isopropanol/acetic acid (v/v, 4:1) |
20 |
150 |
80 |
100 |
70.0 |
12 |
isopropanol/acetic acid (v/v, 4:1) |
360 |
reflux |
0 |
0 |
33.5 |