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. 2012 Jul 2;10(7):1445–1458. doi: 10.3390/md10071445

Table 2.

13C NMR data (CDCl3, δ in ppm) of compounds 17.

C 1 a 2 b 3 a 4 a 5 b 6 a 7 a
s- trans s- cis s- trans s- cis s- trans s- cis s- trans s- cis s- trans s- cis s- trans s- cis s- cis s- trans
1 48.8 45.3 49.0 45.7 45.6 41.1 48.4 45.0 48.8 46.1 40.1 40.1 40.9 45.4
2 22.8 23.1 22.9 23.4 19.1 19.5 22.7 23.1 23.3 23.7 24.6 24.7 18.8 19.1
3 30.96 31.04 30.8 30.9 31.3 31.4 30.8 30.9 30.5 30.6 30.5 30.6 31.1 31.2
4 134.4 134.1 134.9 134.6 134.3 134.2 134.8 134.3 132.4 131.9 131.1 130.8 134.5 134.4
5 123.3 123.8 121.8 122.3 124.3 124.0 122.3 122.7 125.7 126.2 127.1 127.3 123.9 124.2
6 39.5 39.4 38.4 38.2 35.2 34.8 38.6 38.4 39.5 39.2 36.5 36.5 37.0 36.5
7 50.3 50.3 44.6 44.4 42.3 42.0 45.2 45.2 51.2 50.4 44.9 45.2 43.3 43.6
8 29.7 29.9 20.9 20.9 20.1 19.9 25.7 25.8 24.5 24.7 29.48 29.51 28.4 28.4
9 42.0 37.6 41.8 37.4 33.0 33.7 41.7 37.3 42.1 37.8 120.2 120.5 33.5 32.8
10 55.5 57.2 55.6 57.3 55.5 57.1 55.3 56.8 55.4 56.9 136.9 136.8 56.8 55.4
11 151.3 151.9 30.8 30.8 31.3 31.1 62.33 62.7 76.9 77.2 86.4 86.3 139.4 139.0
12 34.2 34.2 35.65 35.69 35.7 35.8 62.27 62.33 31.0 31.7 37.2 37.1 118.6 118.9
13 26.3 26.3 26.2 26.2 26.2 26.3 27.0 27.0 25.9 26.1 25.6 25.8 29.6 29.6
14 124.2 124.3 124.6 124.8 124.7 124.9 119.3 119.5 64.2 64.5 84.2 84.5 77.2 76.8
15 131.7 131.6 131.3 131.1 131.2 131.1 134.2 134.1 74.2 74.4 54.5 55.9 145.4 145.3
16 25.7 25.7 25.7 25.7 25.7 25.7 25.7 25.7 29.7 29.7 27.4 25.1 110.5 110.6
17 17.8 17.8 17.7 17.7 17.7 17.7 18.0 18.0 28.9 28.4 23.8 21.7 18.9 18.9
18 110.0 109.6 13.3 13.3 13.3 13.3 18.5 18.5 21.9 21.2 20.3 21.1 67.63 67.58
19 23.3 23.4 23.6 23.7 23.5 23.4 23.55 23.60 23.8 23.8 23.92 23.87 23.3 23.4
20 19.0 18.9 18.8 18.7 27.2 23.7 18.9 18.7 19.0 18.5 21.53 21.47 23.6 29.7
21 162.8 160.4 163.1 160.5 162.8 160.0 162.8 160.4 162.7 160.4 163.1 160.9 160.1 162.8

a Measured at 125 MHz; b Measured at 100 MHz.