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. 2012 Apr 16;287(30):24916–24928. doi: 10.1074/jbc.M111.316497

TABLE 1.

Data collection and refinement statistics

The hOGG1 dDXL G-complex was space group, P6522; cell parameters, a = b = 90.91 Å, c = 211.63 Å, α = β = 90.0°, and γ = 120°.

Data collectiona
Source APS 24ID
Wavelength (Å) 0.97921
Resolution (Å) 50.0-3.1 (3.21-3.1)
Rsym (%)a 11.3 (54.5)
Total No. of obs. 131,064
No. of unique obs. 10,056 (974)
Completeness (%) 100.0 (99.7)
I〉/σ〈I〉 21.2 (2.6)
Refinement

Resolution (Å) 32.19-3.1
No. reflections 9,362
No. of non-hydrogen atoms 3023
Rwork (%)b 22.84
Rfree (%)c 26.73
Root mean square deviation bond (Å)d 0.002
Root mean square deviation angle (°)d 0.579
Ramachandran plot analysise (% favored, allowed, outlier) 95.1, 4.5, 0.3
Average B-factors Protein, 67.5; DNA, 130.1

a Rsym = Σ|I − 〈I〉|/ΣI, where I is the integrated intensity of a given reflection.

b Rwork = Σ|FobsFcalc|/ΣFobs.

c Rfree = Σ|FobsFcalc|/ΣFobs, calculated using 7.5% of the data.

d From PHENIX (49).

e From PROCHECK (RAMPAGE (65) in the Procheck program in CCP4 (67)).