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Enzymatic generation of 5 by incubating 3 with OleV and OleW. Aliquots (50 μL) were sampled at different time points and analyzed by HPLC. A) Zero time point; B) 1 h; C) overnight. The peak marked with an asterisk is ADP (product from the TTP regeneration system, see Scheme S1 in the Supporting Information).
