Table 4. Data-collection and refinement statistics for FtHAP.
Values in parentheses are for the outer resolution shell.
| Cryoprotectant | 2.0M proline | 20% glycerol |
|---|---|---|
| Space group | P41 | P41 |
| Unit-cell parameters () | a = b = 62.0, c = 210.4 | a = b = 62.0, c = 211.0 |
| Wavelength () | 1.00 | 1.00 |
| Resolution () | 48.61.75 (1.841.75) | 46.51.75 (1.841.75) |
| No. of observations | 341312 | 308938 |
| Unique reflections | 78960 | 76942 |
| R merge(I) | 0.032 (0.130) | 0.065 (0.153) |
| R meas(I) | 0.036 (0.160) | 0.072 (0.199) |
| R p.i.m.(I) | 0.015 (0.092) | 0.030 (0.126) |
| Mean I/(I) | 25.8 (5.7) | 13.1 (3.1) |
| Completeness (%) | 99.1 (95.3) | 96.6 (81.1) |
| Multiplicity | 4.3 (2.8) | 4.0 (1.9) |
| Mosaicity () | 0.18 | 0.24 |
| No. of protein atoms | 5035 | |
| No. of water molecules | 365 | |
| No. of proline molecules | 2 | |
| R cryst | 0.182 | |
| R free † | 0.203 | |
| R.m.s. deviations‡ | ||
| Bond lengths () | 0.006 | |
| Bond angles () | 1.007 | |
| Ramachandran plot§, residues in | ||
| Favored regions | 648 | |
| Allowed regions | 6 | |
| Outliers | 0 | |
| Average B factor (2) | ||
| Protein | 19 | |
| Water | 23 | |
| Proline | 24 | |
| PDB code | 4e3w | |