Table 5. Data-collection and refinement statistics for MmP5CDH.
Values in parentheses are for the outer resolution shell.
| Cryoprotectant | 2.4M proline |
|---|---|
| Space group | P212121 |
| Unit-cell parameters () | a = 85.0, b = 93.9, c = 132.4 |
| Wavelength () | 0.979 |
| Resolution () | 45.61.24 (1.311.24) |
| No. of observations | 1144056 |
| Unique reflections | 279378 |
| R merge(I) | 0.051 (0.550) |
| R meas(I) | 0.058 (0.644) |
| R p.i.m.(I) | 0.027 (0.326) |
| Mean I/(I) | 15.0 (2.3) |
| Completeness (%) | 94.1 (87.3) |
| Multiplicity | 4.1 (3.3) |
| Mosaicity () | 0.17 |
| No. of protein atoms | 8304 |
| No. of water molecules | 882 |
| No. of proline molecules | 7 |
| R cryst | 0.155 |
| R free † | 0.180 |
| R.m.s. deviations† | |
| Bond lengths () | 0.005 |
| Bond angles () | 1.078 |
| Ramachandran plot‡, residues in | |
| Favored regions | 1066 |
| Allowed regions | 19 |
| Outliers | 0 |
| Average B factor (2) | |
| Protein | 12 |
| Water | 22 |
| Proline | 18 |
| PDB code | 4e3x |