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. 2012 Jul 4;68(Pt 8):o2310–o2311. doi: 10.1107/S1600536812029340
O1—C10 1.409 (2) C11—H11A 0.9900
O1—H1o 0.871 (10) C11—H11B 0.9900
N1—C9 1.3220 (19) C12—C19 1.461 (2)
N1—C1 1.366 (2) C13—C18 1.382 (2)
N2—C9 1.382 (2) C13—C14 1.393 (2)
N2—N3 1.3850 (17) C14—C15 1.389 (2)
N2—C10 1.481 (2) C14—H14 0.9500
N3—C12 1.290 (2) C15—C16 1.381 (2)
C1—C2 1.411 (2) C15—H15 0.9500
C1—C6 1.421 (2) C16—C17 1.382 (2)
C2—C3 1.371 (2) C16—H16 0.9500
C2—H2 0.9500 C17—C18 1.383 (2)
C3—C4 1.405 (2) C17—H17 0.9500
C3—H3 0.9500 C18—H18 0.9500
C4—C5 1.367 (2) C19—C24 1.400 (2)
C4—H4 0.9500 C19—C20 1.405 (2)
C5—C6 1.407 (2) C20—C21 1.380 (2)
C5—H5 0.9500 C20—H20 0.9500
C6—C7 1.426 (2) C21—C22 1.386 (2)
C7—C8 1.350 (2) C21—H21 0.9500
C7—H7 0.9500 C22—C23 1.381 (2)
C8—C9 1.429 (2) C22—H22 0.9500
C8—H8 0.9500 C23—C24 1.389 (2)
C10—C13 1.518 (2) C23—H23 0.9500
C10—C11 1.543 (2) C24—H24 0.9500
C11—C12 1.503 (2)
C10—O1—H1o 104 (2) C12—C11—H11B 111.1
C9—N1—C1 117.48 (13) C10—C11—H11B 111.1
C9—N2—N3 119.53 (12) H11A—C11—H11B 109.1
C9—N2—C10 123.18 (12) N3—C12—C19 120.74 (14)
N3—N2—C10 113.46 (12) N3—C12—C11 113.60 (14)
C12—N3—N2 108.27 (13) C19—C12—C11 125.63 (14)
N1—C1—C2 118.47 (14) C18—C13—C14 118.91 (14)
N1—C1—C6 122.77 (14) C18—C13—C10 121.07 (14)
C2—C1—C6 118.76 (14) C14—C13—C10 119.93 (14)
C3—C2—C1 120.37 (15) C15—C14—C13 120.18 (15)
C3—C2—H2 119.8 C15—C14—H14 119.9
C1—C2—H2 119.8 C13—C14—H14 119.9
C2—C3—C4 120.71 (15) C16—C15—C14 120.13 (16)
C2—C3—H3 119.6 C16—C15—H15 119.9
C4—C3—H3 119.6 C14—C15—H15 119.9
C5—C4—C3 120.08 (15) C15—C16—C17 119.90 (16)
C5—C4—H4 120.0 C15—C16—H16 120.1
C3—C4—H4 120.0 C17—C16—H16 120.1
C4—C5—C6 120.68 (16) C16—C17—C18 119.89 (16)
C4—C5—H5 119.7 C16—C17—H17 120.1
C6—C5—H5 119.7 C18—C17—H17 120.1
C5—C6—C1 119.40 (14) C13—C18—C17 120.99 (15)
C5—C6—C7 123.54 (15) C13—C18—H18 119.5
C1—C6—C7 117.06 (14) C17—C18—H18 119.5
C8—C7—C6 120.24 (15) C24—C19—C20 119.05 (14)
C8—C7—H7 119.9 C24—C19—C12 120.41 (14)
C6—C7—H7 119.9 C20—C19—C12 120.51 (15)
C7—C8—C9 118.28 (14) C21—C20—C19 120.14 (15)
C7—C8—H8 120.9 C21—C20—H20 119.9
C9—C8—H8 120.9 C19—C20—H20 119.9
N1—C9—N2 115.56 (14) C20—C21—C22 120.45 (15)
N1—C9—C8 124.12 (14) C20—C21—H21 119.8
N2—C9—C8 120.31 (14) C22—C21—H21 119.8
O1—C10—N2 110.25 (13) C23—C22—C21 119.90 (15)
O1—C10—C13 111.82 (12) C23—C22—H22 120.1
N2—C10—C13 111.52 (13) C21—C22—H22 120.1
O1—C10—C11 108.52 (13) C22—C23—C24 120.55 (16)
N2—C10—C11 100.60 (12) C22—C23—H23 119.7
C13—C10—C11 113.56 (13) C24—C23—H23 119.7
C12—C11—C10 103.23 (13) C23—C24—C19 119.88 (15)
C12—C11—H11A 111.1 C23—C24—H24 120.1
C10—C11—H11A 111.1 C19—C24—H24 120.1
C9—N2—N3—C12 −165.92 (14) N2—C10—C11—C12 −7.55 (15)
C10—N2—N3—C12 −7.26 (17) C13—C10—C11—C12 −126.82 (14)
C9—N1—C1—C2 −178.59 (14) N2—N3—C12—C19 −176.76 (13)
C9—N1—C1—C6 2.3 (2) N2—N3—C12—C11 1.48 (18)
N1—C1—C2—C3 −178.78 (14) C10—C11—C12—N3 4.29 (18)
C6—C1—C2—C3 0.4 (2) C10—C11—C12—C19 −177.58 (14)
C1—C2—C3—C4 −0.2 (2) O1—C10—C13—C18 −153.52 (15)
C2—C3—C4—C5 −0.1 (2) N2—C10—C13—C18 −29.6 (2)
C3—C4—C5—C6 0.2 (2) C11—C10—C13—C18 83.26 (19)
C4—C5—C6—C1 0.0 (2) O1—C10—C13—C14 30.0 (2)
C4—C5—C6—C7 179.05 (15) N2—C10—C13—C14 153.99 (14)
N1—C1—C6—C5 178.84 (14) C11—C10—C13—C14 −93.20 (18)
C2—C1—C6—C5 −0.3 (2) C18—C13—C14—C15 0.1 (2)
N1—C1—C6—C7 −0.3 (2) C10—C13—C14—C15 176.68 (15)
C2—C1—C6—C7 −179.38 (14) C13—C14—C15—C16 0.6 (3)
C5—C6—C7—C8 179.68 (15) C14—C15—C16—C17 −0.6 (3)
C1—C6—C7—C8 −1.3 (2) C15—C16—C17—C18 −0.1 (3)
C6—C7—C8—C9 0.7 (2) C14—C13—C18—C17 −0.9 (2)
C1—N1—C9—N2 175.86 (13) C10—C13—C18—C17 −177.38 (15)
C1—N1—C9—C8 −2.9 (2) C16—C17—C18—C13 0.9 (3)
N3—N2—C9—N1 165.54 (13) N3—C12—C19—C24 171.36 (14)
C10—N2—C9—N1 9.0 (2) C11—C12—C19—C24 −6.6 (2)
N3—N2—C9—C8 −15.6 (2) N3—C12—C19—C20 −6.8 (2)
C10—N2—C9—C8 −172.13 (14) C11—C12—C19—C20 175.19 (15)
C7—C8—C9—N1 1.5 (2) C24—C19—C20—C21 −1.5 (2)
C7—C8—C9—N2 −177.26 (14) C12—C19—C20—C21 176.65 (15)
C9—N2—C10—O1 52.69 (19) C19—C20—C21—C22 0.0 (2)
N3—N2—C10—O1 −105.08 (14) C20—C21—C22—C23 1.3 (3)
C9—N2—C10—C13 −72.15 (18) C21—C22—C23—C24 −0.9 (3)
N3—N2—C10—C13 130.07 (13) C22—C23—C24—C19 −0.7 (2)
C9—N2—C10—C11 167.12 (14) C20—C19—C24—C23 1.9 (2)
N3—N2—C10—C11 9.34 (16) C12—C19—C24—C23 −176.29 (14)
O1—C10—C11—C12 108.17 (14)