Bruker APEX DUO CCD diffractometer | 7190 independent reflections |
Radiation source: fine-focus sealed tube | 6068 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.045 |
φ and ω scans | θmax = 34.8°, θmin = 1.7° |
Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −25→25 |
Tmin = 0.954, Tmax = 0.990 | k = −28→28 |
97212 measured reflections | l = −18→18 |