Nonius KappaCCD diffractometer | 5194 independent reflections |
Radiation source: fine-focus sealed tube | 3970 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.031 |
Thin slice ω and φ scans | θmax = 27.5°, θmin = 3.6° |
Absorption correction: multi-scan (SORTAV; Blessing, 1995) | h = −25→22 |
Tmin = 0.910, Tmax = 0.991 | k = −7→8 |
20137 measured reflections | l = −25→25 |