Rigaku AFC10/Saturn724+ diffractometer	4194 reflections with I > 2σ(I)
Radiation source: Rotating Anode	Rint = 0.047
Graphite monochromator	θmax = 29.1°, θmin = 2.4°
Detector resolution: 28.5714 pixels mm-1	h = −10→12
φ and ω scans	k = −11→12
25322 measured reflections	l = −57→43
4876 independent reflections