Table 1.
X-ray data collection statisticsa
| X-ray statistic | Value for indicated PDB entry |
|||
|---|---|---|---|---|
| 4AWY | 4AWZ | 4AX0 | 4AX1 | |
| Beamline | ID29 | ID29 | I911-3 | I911-3 |
| Space group | P6122 | P61 | P6122 | P6122 |
| Unit cell (Å) | a = b = 77.83; c = 239.02 | a = b = 79.47; c = 229.27 | a = b = 78.04; c = 239.48 | a = b = 77.99; c = 239.77 |
| Resolution (Å) (highest bin) | 28-1.60 (1.68-1.60) | 30-1.80 (1.90-1.80) | 30-1.83 (1.83-1.73) | 30-1.40 (1.40-1.48) |
| Wavelength (Å) | 1.23985 | 1.10481 | 1.0000 | 1.0000 |
| No. of unique reflections | 56,470 | 74,731 | 43,793 | 82,502 |
| Multiplicity | 5.5 (3.9) | 5.0 (4.8) | 4.4 (2.3) | 6.4 (3.4) |
| Completeness (%) | 97.8 (87.0) | 98.9 (99.6) | 96.2 (76.4) | 96.3 (76.7) |
| Mean (<I>/<σI>) | 20.3 (6.6) | 17.5 (4.0) | 9.3 (2.0) | 10.5 (2.1) |
| Rmerge (%)b | 4.6 (13.8) | 7.3 (37.8) | 8.0 (45.7) | 8.6 (46.0) |
| Wilson B-factor (Å2) | 14.57 | 12.84 | 17.06 | 15.21 |
a
Numbers in parentheses represent values for the highest of 10 resolution shells except where indicated.
b
Rmerge = [ΣhΣi | Ii (h) − <I(h)>|)/(ΣhΣI I(h)], where Ii(h) is the i-th measurement of reflection h and <I(h)> is the weighted mean of all measurements of h.