Table 2. Graphite furnace programme.
Step | T (°C) | Ramp (s) | Hold (s) | Flow (mL/min) |
1 | 90 | 5 | 10 | 250 |
2 | 110 | 3 | 20 | 250 |
3 | 300 | 20 | 10 | 250 |
4 | 1100 | 30 | 20 | 250 |
5 | 1200 | 1 | 2 | 0 |
6 | 2100 | 0 | 4 | 0 |
7 | 2300 | 1 | 4 | 250 |
Step | T (°C) | Ramp (s) | Hold (s) | Flow (mL/min) |
1 | 90 | 5 | 10 | 250 |
2 | 110 | 3 | 20 | 250 |
3 | 300 | 20 | 10 | 250 |
4 | 1100 | 30 | 20 | 250 |
5 | 1200 | 1 | 2 | 0 |
6 | 2100 | 0 | 4 | 0 |
7 | 2300 | 1 | 4 | 250 |