Bruker SMART APEXII area-detector diffractometer | 4918 independent reflections |
Radiation source: fine-focus sealed tube | 4859 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.025 |
0.50° ω and 0.5 ° φ scans | θmax = 69.8°, θmin = 4.7° |
Absorption correction: analytical (SADABS; Sheldrick, 2003) | h = −10→11 |
Tmin = 0.611, Tmax = 0.867 | k = −19→19 |
22577 measured reflections | l = −11→11 |