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. 2012 Aug 23;68(Pt 9):o2757–o2758. doi: 10.1107/S160053681203601X
Bruker SMART APEXII area-detector diffractometer 4918 independent reflections
Radiation source: fine-focus sealed tube 4859 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.025
0.50° ω and 0.5 ° φ scans θmax = 69.8°, θmin = 4.7°
Absorption correction: analytical (SADABS; Sheldrick, 2003) h = −10→11
Tmin = 0.611, Tmax = 0.867 k = −19→19
22577 measured reflections l = −11→11