Refinement on F2
|
Secondary atom site location: difference Fourier map |
Least-squares matrix: full |
Hydrogen site location: inferred from neighbouring sites |
R[F2 > 2σ(F2)] = 0.025 |
H atoms treated by a mixture of independent and constrained refinement |
wR(F2) = 0.065 |
w = 1/[σ2(Fo2) + (0.0447P)2 + 0.2408P] where P = (Fo2 + 2Fc2)/3 |
S = 1.02 |
(Δ/σ)max = 0.001 |
4918 reflections |
Δρmax = 0.29 e Å−3
|
343 parameters |
Δρmin = −0.15 e Å−3
|
1 restraint |
Absolute structure: Flack (1983), 2188 Friedel pairs |
Primary atom site location: structure-invariant direct methods |
Flack parameter: 0.022 (9) |