| Agilent Xcalibur Atlas CCD-detector diffractometer | 2862 independent reflections |
| Radiation source: fine-focus sealed tube | 2229 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.025 |
| Detector resolution: 10.3088 pixels mm-1 | θmax = 25.0°, θmin = 2.7° |
| ω scans | h = −14→16 |
| Absorption correction: multi-scan (CrysAlis PRO; Agilent, 2010) | k = −9→8 |
| Tmin = 0.900, Tmax = 1.000 | l = −18→18 |
| 8931 measured reflections |
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