TABLE 2.

Proton assignments for 8-hydroxy-benzo[a]pyrene-7-O-sulfate

m, multiplet; d, doublet; and s, singlet.

Proton	Chemical shift, multiplicity	Coupling constants (Hz)	Connectivities
	ppm	J
H-1 or H3	8.08, d; 8.22, d	7.7 or 7.8	H-2 with H-1/H-3
H-2	7.95, m		H-1/H-3 with H-2
H-4	7.92, m		H-4 with H-5
H-5	8.05, d	9.1	H-5 with H-4
H-6	8.88, s
H-9	7.52, d	9.3	H-9 with H-10
H-10	8.88, d	9.1	H-10 with H-9
H-11	9.02, d	9.1	H-11 with H-12
H-12	8.31, d	9.1	H-12 with H-11