Table 1.
Data collection and refinement statistics
| Data collection and process | |
|---|---|
| Beamline | SSRL BL 12-2 |
| Wavelength (Å) | 0.9795 |
| Space group | C2 |
| Unit cell (Å) | 184.1, 132.7, 162.1 |
| β (°) | 103.6 |
| Resolution (Å) | 25-2.99 |
| Rmerge(%)a | 8.3 (59.8) |
| Completeness (%)a | 97.6 (92.3) |
| <I/σ>a | 12.6 (2.2) |
| Unique reflectionsa | 74604 (10257) |
| Redundancya | 3.9 (3.9) |
|
Refinement statistics | |
| Resolution (Å) | 24.8-2.99 |
| No. Reflections (test set) | 68525 (3452) |
| Rwork/Rfeee | 0.187/0.219 |
| Non-H protein (ligand) atoms | 13358 (675) |
| <B-factors> (Å2) | |
| Protein | 70.6 |
| Detergents | 125.0 |
| Lipids | 119.1 |
| Solvent | 51.7 |
| Ketamine | 122.3 |
| R.m.s deviations | |
| Bond lengths (Å) | 0.008 |
| Bond angles (degrees) | 1.22 |
| Rotamer outliers (%) | 8.3 |
| Ramachandran outliers (%) | 0.97 |
| Ramachandran favored (%) | 93.3 |
| PDB code | 4F8H |
a
Values in the parentheses are for highest-resolution shell.