Table 2.
Optimization Au(PPh3)Cl/AgSbF6 Catalyst Loadinga
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---|---|---|---|---|
entry | mol % | temp. °C | time | yield 9 |
1 | 10 | 23 | <5 min | 92 |
2 | 5 | 23 | <10 min | 94 |
3 | 2 | 80 | 1 hr | 94 |
4 | 1 | 80 | 6 hr | 93 |
All reactions were run at a concentration of 0.05M.
Optimization Au(PPh3)Cl/AgSbF6 Catalyst Loadinga
![]() | ||||
---|---|---|---|---|
entry | mol % | temp. °C | time | yield 9 |
1 | 10 | 23 | <5 min | 92 |
2 | 5 | 23 | <10 min | 94 |
3 | 2 | 80 | 1 hr | 94 |
4 | 1 | 80 | 6 hr | 93 |
All reactions were run at a concentration of 0.05M.