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. Author manuscript; available in PMC: 2012 Sep 25.
Published in final edited form as: J Nat Prod. 2008 Sep 23;71(10):1749–1753. doi: 10.1021/np800328r

Table 1.

13C NMR Data for Compounds 1–4 in Pyridine-d5 and 8 in CDCl3 (δ, ppm)a

position 1 2 3 4 8
1 72.0 d 210.7 s 205.6 s 200.9 s 200.6 s
2 31.8 t 48.8 t 47.3 t 129.6 d 126.3 d
3 77.0 d 78.5 d 80.5 d 159.1 d 159.8 d
4 37.7 s 39.9 s 40.8 s 37.0 s 36.8 s
5 46.1 d 38.7 d 43.8 d 42.5 d 44.8 d
6 30.9 t 31.5 t 30.8 t 31.5 t 35.3 t
7 75.8 d 68.4 d 23.8 t 68.0 d 72.0 d
8 53.1 d 51.5 d 39.6 d 52.8 d 55.4 d
9 135.9 s 28.7 s 33.5 s 31.9 s 133.5 s
10 84.8 s 39.4 s 48.6 s 35.9 s 47.1 d
11 121.1 d 29.2 t 209.3 s 25.8 t 127.3 d
12 37.6 t 33.6 t 52.6 t 34.9 t 37.7 t
13 45.7 s 45.9 s 46.7 s 45.8 s 45.5 s
14 45.4 s 50.1 s 49.3 s 49.8 s 48.4 s
15 34.4 t 34.5 t 34.2 t 33.4 t 28.9 t
16 28.8 t 28.4 t 28.4 t 29.6 t 28.5 t
17 51.0 d 52.4 d 51.7 d 52.5 d 50.4 d
18 15.5 q 16.0 q 17.0 q 16.3 q 15.2 q
19 42.8 t 24.4 t 25.6 t 29.1 t 33.8 t
20 37.2 d 37.4 d 37.2 d 37.5 d 36.6 d
21 19.2 q 19.3 q 19.3 q 19.3 q 18.7 q
22 35.0 t 34.9 t 34.7 t 34.9 t 39.4 t
23 29.6 t 29.5 t 29.6 t 28.5 t 33.7 t
24 78.7 d 78.7 d 78.6 d 78.7 d 79.7 d
25 81.3 s 81.3 s 81.3 s 81.3 s 73.4 s
26 21.7 q 21.6 q 21.7 q 21.6 q 23.4 q
27 24.6 q 24.6 q 24.6 q 24.6 q 26.7 q
28 27.4 q 25.6 q 26.0 q 28.0 q 27.9 q
29 24.0 q 21.7 q 21.5 q 21.4 q 20.0 q
30 20.0 q 18.9 q 19.1 q 19.1 q 18.4 q
1′ 99.0 d 99.0 d 99.1 d 99.0 d
2′ 75.7 d 75.7 d 75.7 d 75.7 d
3′ 79.0 d 79.0 d 79.1 d 79.0 d
4′ 72.1 d 72.0 d 72.1 d 72.0 d
5′ 78.6 d 78.4 d 78.7 d 78.6 d
6′ 63.1 t 63.0 t 63.1 t 63.0 t
a

Spectra were acquired at 150 MHz for 1 and 100 MHz for 2–4 and 8. Multiplicity was obtained from DEPT spectra.