Table 1.
position | 1 | 2 | 3 | 4 | 8 | |||||
---|---|---|---|---|---|---|---|---|---|---|
1 | 72.0 | d | 210.7 | s | 205.6 | s | 200.9 | s | 200.6 | s |
2 | 31.8 | t | 48.8 | t | 47.3 | t | 129.6 | d | 126.3 | d |
3 | 77.0 | d | 78.5 | d | 80.5 | d | 159.1 | d | 159.8 | d |
4 | 37.7 | s | 39.9 | s | 40.8 | s | 37.0 | s | 36.8 | s |
5 | 46.1 | d | 38.7 | d | 43.8 | d | 42.5 | d | 44.8 | d |
6 | 30.9 | t | 31.5 | t | 30.8 | t | 31.5 | t | 35.3 | t |
7 | 75.8 | d | 68.4 | d | 23.8 | t | 68.0 | d | 72.0 | d |
8 | 53.1 | d | 51.5 | d | 39.6 | d | 52.8 | d | 55.4 | d |
9 | 135.9 | s | 28.7 | s | 33.5 | s | 31.9 | s | 133.5 | s |
10 | 84.8 | s | 39.4 | s | 48.6 | s | 35.9 | s | 47.1 | d |
11 | 121.1 | d | 29.2 | t | 209.3 | s | 25.8 | t | 127.3 | d |
12 | 37.6 | t | 33.6 | t | 52.6 | t | 34.9 | t | 37.7 | t |
13 | 45.7 | s | 45.9 | s | 46.7 | s | 45.8 | s | 45.5 | s |
14 | 45.4 | s | 50.1 | s | 49.3 | s | 49.8 | s | 48.4 | s |
15 | 34.4 | t | 34.5 | t | 34.2 | t | 33.4 | t | 28.9 | t |
16 | 28.8 | t | 28.4 | t | 28.4 | t | 29.6 | t | 28.5 | t |
17 | 51.0 | d | 52.4 | d | 51.7 | d | 52.5 | d | 50.4 | d |
18 | 15.5 | q | 16.0 | q | 17.0 | q | 16.3 | q | 15.2 | q |
19 | 42.8 | t | 24.4 | t | 25.6 | t | 29.1 | t | 33.8 | t |
20 | 37.2 | d | 37.4 | d | 37.2 | d | 37.5 | d | 36.6 | d |
21 | 19.2 | q | 19.3 | q | 19.3 | q | 19.3 | q | 18.7 | q |
22 | 35.0 | t | 34.9 | t | 34.7 | t | 34.9 | t | 39.4 | t |
23 | 29.6 | t | 29.5 | t | 29.6 | t | 28.5 | t | 33.7 | t |
24 | 78.7 | d | 78.7 | d | 78.6 | d | 78.7 | d | 79.7 | d |
25 | 81.3 | s | 81.3 | s | 81.3 | s | 81.3 | s | 73.4 | s |
26 | 21.7 | q | 21.6 | q | 21.7 | q | 21.6 | q | 23.4 | q |
27 | 24.6 | q | 24.6 | q | 24.6 | q | 24.6 | q | 26.7 | q |
28 | 27.4 | q | 25.6 | q | 26.0 | q | 28.0 | q | 27.9 | q |
29 | 24.0 | q | 21.7 | q | 21.5 | q | 21.4 | q | 20.0 | q |
30 | 20.0 | q | 18.9 | q | 19.1 | q | 19.1 | q | 18.4 | q |
1′ | 99.0 | d | 99.0 | d | 99.1 | d | 99.0 | d | ||
2′ | 75.7 | d | 75.7 | d | 75.7 | d | 75.7 | d | ||
3′ | 79.0 | d | 79.0 | d | 79.1 | d | 79.0 | d | ||
4′ | 72.1 | d | 72.0 | d | 72.1 | d | 72.0 | d | ||
5′ | 78.6 | d | 78.4 | d | 78.7 | d | 78.6 | d | ||
6′ | 63.1 | t | 63.0 | t | 63.1 | t | 63.0 | t |
Spectra were acquired at 150 MHz for 1 and 100 MHz for 2–4 and 8. Multiplicity was obtained from DEPT spectra.