Table 4.
Assignment of some bands of CAMB after freeze drying and after storage (cm−1)
Assignment of functional group | Frequency (cm−1) in: |
||||
---|---|---|---|---|---|
CAMB after FD | CAMB (aw, 0.07) | CAMB (aw, 0.1) | CAMB (aw, 0.2) | CAMB in aluminum foil | |
P![]() |
1,043.6 ± 0.5 | 1,043.8 ± 0.2 | 1,042.3 ± 0.3 | 1,043.2 ± 0.3 | 1,047.4 ± 0.4 |
P![]() |
1,218.5 ± 0.5 | 1,226.5 ± 0.5 | 1,225.2 ± 0.3 | 1,226.2 ± 0.3 | 1,227.2 ± 0.3 |
N+(CH3)3 asymmetric stretching | 978.2 ± 0.3 | 979.8 ± 0.3 | 983.8 ± 0.3 | 994.7 ± 0.3 | 995.9 ± 0.2 |
CH2 symmetric stretching | 2,867.4 ± 0.1 | 2,854.3 ± 0.6 | 2,855.5 ± 0.5 | 2,853.2 ± 0.3 | 2,849.0 ± 0.0 |
CH2 asymmetric stretching | 2,923.3 ± 0.2 | 2,920.7 ± 0.6 | 2,921.5 ± 0.6 | 2,920.7 ± 0.6 | 2,931.5 ± 0.5 |
Amide II | 1,536.4 ± 0.4 | 1,534.5 ± 0.5 | 1,537.8 ± 0.3 | 1,536.5 ± 0.5 | 1,529.8 ± 0.3 and 1,515 ± 0.1 |