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. Author manuscript; available in PMC: 2013 Sep 17.
Published in final edited form as: Inorg Chem. 2012 Sep 4;51(18):9852–9864. doi: 10.1021/ic301289j

Table 3.

NMR Spectroscopic Data for [1]2+–[3]2+a

1H 13C 14N 195Pt
compound δ NH3, ppm 1JNH, Hz δ CH3CO2− δ NH3, ppm δ, ppm 1JNPt, Hz
[1]2+ 5.07 n.o.b 185.9 −86 −1401 n.o.b
[2]2+ 6.44 49 195.2 −65 −76 226
[3]2+ 6.43 44 196.2 −67 −216 232
a

All spectra were acquired at room temperature in DMF-d7.

b

Not observed under these experimental conditions.