Table 3.
entry | R2 | yield of 3a (%) | purityb | |
1 | 9{1,3} | 48 3{1,3} | 99% | |
2 | 9{1,4} | 46 3{1,4} | 99% |
aIsolated yields; bpurity determined by LCMS/ELS.
entry | R2 | yield of 3a (%) | purityb | |
1 | 9{1,3} | 48 3{1,3} | 99% | |
2 | 9{1,4} | 46 3{1,4} | 99% |
aIsolated yields; bpurity determined by LCMS/ELS.