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. 2012 Jul 10;8:1048–1058. doi: 10.3762/bjoc.8.117

Table 3.

Synthesis of α-methylenecyclopentenone library 3{1,3}3{1,4}.

graphic file with name Beilstein_J_Org_Chem-08-1048-i027.jpg

entry R2 yield of 3a (%) purityb

1 graphic file with name Beilstein_J_Org_Chem-08-1048-i028.jpg 9{1,3} 48 3{1,3} 99%
2 graphic file with name Beilstein_J_Org_Chem-08-1048-i029.jpg 9{1,4} 46 3{1,4} 99%

aIsolated yields; bpurity determined by LCMS/ELS.