Table 1.
Data collection and refinement statisticsa
| RSK2-SL0101 | RSK2-Afzelin | |
|---|---|---|
| Data collection | ||
| Space group | C2 | C2 |
| Cell dimensions | ||
| a, b, c (Å) | 98.45, 40.70, 83.35 | 99.12, 40.86, 83.87 |
| β (°) | 114.54 | 114.65 |
| Resolution (Å) | 1.53 (1.56–1.53)b | 1.55 (1.58–1.55) |
| Number of unique reflections | 46201 (2182) | 43194 (1739) |
| Rsym | 0.062 (0.471) | 0.053 (0.355) |
| <I /σ(I)> | 24.0 (2.2) | 23.2 (2.0) |
| Completeness (%) | 99.5 (95.1) | 96.8 (76.9) |
| Redundancy | 4.5 (2.7) | 4.1 (2.2) |
| Refinement | ||
| Resolution (Å) | 1.53 | 1.55 |
| No. reflections | 44706 | 41260 |
| Rwork / Rfree | 0.19/0.22 | 0.20/0.23 |
| No. atoms | ||
| Protein (non-hydrogen) | 2364 | 2354 |
| Inhibitor (all atoms) | 60 | 50 |
| Water | 337 | 285 |
| B-factors (Å2) | ||
| Protein | 26.1 | 26.4 |
| Inhibitor | 26.0 | 22.9 |
| Water | 34.5 | 32.8 |
| R.m.s. deviations | ||
| Bond lengths (Å) | 0.006 | 0.006 |
| Bond angles (°) | 0.97 | 0.94 |
a
Each dataset was collected from one native crystal
b
Values in parentheses are for highest-resolution shell.