Table 3.

Table of NMR chemical shifts

DOI: http://dx.doi.org/10.7554/eLife.00013.024

Position	δ 1H (multiplicity, J, #H)	13C (δ, ppm)
NH	8.21 (d, J=9.1 Hz, 1H)
1	3.01 (dd, J=14.2, 5.1 Hz, 1H)	51.87
	2.56 (dd, J=14.3, 3.6 Hz, 1H)
2	3.88 (ddd, J=13.0, 8.6, 4.5 Hz, 1H)	50.89
3	3.78 – 3.71 (m, 1H)	71.51
OH3	5.20 (d, J=4.2 Hz, 1H)
4	1.51 – 1.47 (m, 1H)	41.36
	1.33 – 1.29 (m, 1H)
5	3.61 – 3.53 (m, 1H)	70.20
OH5	4.31 (d, J=3.5 Hz, 1H)
6	1.34 – 1.29 (m, 1H)	37.27
	1.24 – 1.20 (m, 1H)
7–13	1.21 – 1.27 (br s, 14H)	22.5–29.6
14	1.16 – 1.11 (m, 2H)	38.91
15	1.52 – 1.47 (m, 1H)	27.79
16, 17	0.84 (d, J=6.6 Hz, 6H)	22.09
1′		173.23
2′	3.80 (dd, J=6.6, 4.2 Hz, 1H)	71.29
OH2′	5.52 (d, J=5.0 Hz, 1H)
3′	1.59 – 1.54 (m, 1H)	34.85
	1.50 – 1.45 (m, 1H)
4′?	1.35 – 1.30 (m, 2H)	24.99
5′–11′	1.21 – 1.27 (br s, 14H)	22.5–29.6
12′	1.16 – 1.11 (m, 2H)	38.91
13′	1.52 – 1.47 (m, 1H)	27.79
14′, 15′	0.84 (d, J=6.6 Hz, 6H)	22.09