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. Author manuscript; available in PMC: 2013 Oct 1.
Published in final edited form as: Inorg Chem. 2012 Sep 18;51(19):10274–10278. doi: 10.1021/ic301241s

Figure 1.

Figure 1

Solid-state structures for (a) (PhL)Fe3Cl(py) (3), (b) [(PhL)Fe3(µ-Br)]2 (4), and (c) (PhL)Fe3I(thf) (6) with the thermal ellipsoids set at the 50% probability level (hydrogen atoms, and solvent molecules omitted for clarity; Fe orange, C black, H white, N blue, O red, Cl green, Br brown, I magenta). Bond lengths (Å) for 3: Fe1-Fe2, 2.7303(8); Fe1-Fe3, 2.6534(8); Fe2-Fe3, 2.2955(8); Fe1-Cl, 2.3333(11); Fe1-Npy, 2.066(3); for 4: Fe1-Fe2, 2.5871(7); Fe1-Fe3, 2.5873(7); Fe2-Fe3, 2.3504(7); Fe1-Br1, 2.5715(6), Fe1-Br2, 2.4670(6); Fe1-Fe1, 3.5810(11); for 6: Fe1-Fe2, 2.6026(10); Fe1-Fe3, 2.6971(11); Fe2-Fe3, 2.3079(10); Fe1-I, 2.6695(9); Fe1-O, 2.024(4).