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. Author manuscript; available in PMC: 2013 Aug 28.
Published in final edited form as: Organometallics. 2012 Jul 25;31(16):5772–5781. doi: 10.1021/om3006239

Table 1.

Selected Structural Parameters of complex 3 obtained from X-ray single crystal diffraction studies. Bond lengths in Å and angles in °.

Pd(1)-C(18) 1.966(4) C(18)-Pd(1)-O(1) 92.08(15)
Pd(1)-O(1) 2.023(3) C(18)-Pd(1)-N(1) 81.35(16)
Pd(1)-N(1) 2.037(4) O(1)-Pd(1)-N(1) 173.02(13)
Pd(1)-O(2) 2.094(3) C(18)-Pd(1)-O(2) 175.51(14)
N(1)-P(1) 1.643(4) O(1)-Pd(1)-O(2) 91.49(12)
O(1)-C(2) 1.289(6) N(1)-Pd(1)-O(2) 94.96(13)
N(1)-C(12) 1.394(6) C(2)-O(1)-Pd(1) 123.3(3)
C(12)-N(1)-P(1) 120.5(3)
C(18)-Pd(1)-O(1) 92.08(15) C(12)-N(1)-Pd(1) 115.8(3)
C(18)-Pd(1)-N(1) 81.35(16) P(1)-N(1)-Pd(1) 123.4(2)