| Agilent Xcalibur Atlas Gemini diffractometer | 8436 independent reflections |
| Radiation source: Enhance (Mo) X-ray Source | 7464 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.034 |
| Detector resolution: 10.4685 pixels mm-1 | θmax = 26.1°, θmin = 3.4° |
| φ and ω scans | h = −9→9 |
| Absorption correction: analytical [CrysAlis PRO (Agilent, 2010); based on expressions derived by Clark & Reid (1995)] | k = −19→19 |
| Tmin = 0.599, Tmax = 0.816 | l = −20→21 |
| 15907 measured reflections |
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