| Agilent Xcalibur Sapphire2 diffractometer | 11118 independent reflections |
| Radiation source: fine-focus sealed tube | 8660 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.041 |
| Detector resolution: 8.2632 pixels mm-1 | θmax = 25.4°, θmin = 2.9° |
| ω scans | h = −17→17 |
| Absorption correction: multi-scan (CrysAlis PRO; Agilent, 2010) | k = −28→28 |
| Tmin = 0.770, Tmax = 1.000 | l = −21→21 |
| 32355 measured reflections |
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