Refinement. This compound, 9940 numbers of reflections were collected and measured during the refinement. Symmetry related reflections were measured more than once and after merging the symmetry equivalent reflections there were only 2783 reflection left. 10 more reflections were filtered, as sigma cutoff was set as 3 and (sinθ/x)set to>0.01 (to eliminate reflection measured near the vicinity of beam stop) therefore numbers of reflection reduced to 2773.