Bruker Kappa DUO APEXII diffractometer | 3497 independent reflections |
Radiation source: fine-focus sealed tube | 2324 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.029 |
0.5° φ scans and ω scans | θmax = 25.0°, θmin = 1.5° |
Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −14→13 |
Tmin = 0.924, Tmax = 0.990 | k = −16→16 |
9454 measured reflections | l = −7→15 |