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. 2012 Sep 22;68(Pt 10):o2977–o2978. doi: 10.1107/S1600536812039451
Bruker Kappa DUO APEXII diffractometer 3497 independent reflections
Radiation source: fine-focus sealed tube 2324 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.029
0.5° φ scans and ω scans θmax = 25.0°, θmin = 1.5°
Absorption correction: multi-scan (SADABS; Bruker, 2008) h = −14→13
Tmin = 0.924, Tmax = 0.990 k = −16→16
9454 measured reflections l = −7→15