Table 4.
Project | Survey years | Limit of detection (LOD) (ng OTA g−1) | Limit of quantification (LOQ) (ng OTA g−1) | Recovery (%)a | Reference |
Canadian Grain Commission (CGC) | 1994–2005 | – | 1 | 88.4 | CGC – TW Nowicki, Personal Communication |
HC – rice | 1993–1995 | −−− | 0.5 | 97.0 | HC – Dr. P Pantazopoulos, Personal Communication |
HC – breakfast cereals | 1999/2000–2001/2002 | 0.05 | 0.2 | 83.3 | Roscoe et al. (2008) |
HC – bran cereals | 2004/2005–2005/2006 | 0.05, 0.2 | 0.2, 0.5 | 93.0 | HC – Dr. P Pantazopoulos, Personal Communication |
HC – infant cereals | 1997/1998–1999/2000 | – | 0.2, 0.5 | 92.0 | Lombaert et al. (2003) |
HC – infant cereals | 1998–1999, 2000–2002 | 0.15 | 0.5 | 96.1 | HC – Ms V Roscoe, Personal Communication |
HC – soy-based infant formula | 2000–2001 | 0.05 | 0.2 | 85.4 | HC – Ms V Roscoe, Personal Communication |
HC – beer | 1995 | 0.05, 0.1 | – | 95.3 | Scott and Kanhere (1995) |
HC – wine and grape juice | 1999/2000–2001/2002 | 0.008b | 0.04b | 87.4 | Ng et al. (2004) |
HC – coffee | 1997–1998 | – | 0.1 | 78.5 | Lombaert et al. (2002) |
HC – dried fruit | 1998/1999–2000/01 | 0.03 | 0.1 | 81.0 | Lombaert et al. (2004) |
HC – pork kidney | 1990–1997 | – | 0.5, 1.0 | 91.7 | HC – Kuiper-Goodman et al, 1993; Mr G Lombaert, Personal Communication |
HC – pasta | 2004–2006 | 0.2, 0.05 | 0.5, 0.2 | 91.0 | Ng et al. (2009) |
Notes: aRecovery is the mean of all recoveries.
White wine had an LOD = 0.004 ng OTA g−1 and an LOQ = 0.02 ng OTA g−1 compared with 0.008 and 0.04 ng OTA g−1 for red wine and grape juice, respectively, indicated above.