Table 3.
Position | 13C-NMR (δC) | 1H-NMR (δH) | JHH(Hz) |
---|---|---|---|
Feruloyl moiety | |||
1 |
169.2 |
- |
- |
2 |
118.8 |
5.82 |
d, J = 12.8 |
3 |
142.0 |
6.61 |
d, J = 12.8 |
4 |
132.1 |
- |
- |
5 |
111.6 |
7.36 |
d, J = 2.0 |
6 |
149.9 |
- |
- |
7 |
149.0 |
- |
- |
8 |
116.5 |
6.73 |
d, J = 8.4 |
9 |
123.2 |
6.93 |
dd, J = 8.4, 2.0 |
OMe |
56.4 |
3.82 |
s |
Methoxytyramine moiety | |||
1´ |
42.5 |
3.49 |
t, J = 7.2 |
2´ |
36.2 |
2.77 |
t, J = 7.2 |
3´ |
128.3 |
- |
- |
4´ |
113.5 |
6.82 |
d, J = 2.0 |
5´ |
149.3 |
- |
- |
6´ |
146.1 |
- |
- |
7´ |
116.2 |
6.63 |
d, J = 8.0 |
8´ |
122.3 |
6.67 |
dd, J = 8.0, 2.0 |
OMe´ | 56.6 | 3.88 | s |