Skip to main content
. Author manuscript; available in PMC: 2013 Oct 15.
Published in final edited form as: J Chromatogr B Analyt Technol Biomed Life Sci. 2012 Sep 18;907:126–139. doi: 10.1016/j.jchromb.2012.09.020

Table 1.

Major phase II metabolites of thiol-conjugated [6]-shogaol in mouse urine.

Compound/metabolite name Peak# Retention time (min)
5-Cys-6S 1 23.10
5-NAC-6S 2 33.50
5-Cys-Gly-6S 3 19.52
5-Methylthio-6S 4 35.34
5-Cys-M6 5 25.48
5-NAC-M6 6 35.39
5-Cys-Gly-M6 7 21.30
5-Methylthio-M6 8 35.73
5-Cys-6S-Glu 9 25.77
5-NAC-6S-Glu 10 35.89
5-Cys-Gly-6S-Glu 11 22.05
5-Methylthio-6S-Glu 12 40.42
5-Cys-M6-Glu 13 24.48
14 28.29
5-Cys-M6-Sul 15 36.46
16 39.30
5-NAC-M6-Glu 17 34.89
18 36.87
5-Cys-Gly-M6-Glu 19 20.91
20 23.98
5-Cys-Gly-M6-Sul 21 27.09
22 30.57
5-Methylthio-M6-Glu 23 36.79
24 40.60