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. Author manuscript; available in PMC: 2013 Oct 1.
Published in final edited form as: Synlett. 2012 Oct;23(17):2539–2543. doi: 10.1055/s-0031-1290461

Table 2.

1,2,3-Triazole-Containing Farnesol Analogues

Entry Compound Structure Yield (%)a Purity LC–MS (%)b
1 4a graphic file with name nihms-411663-t0005.jpg 53 96
2 4b graphic file with name nihms-411663-t0006.jpg 55 89
3 4c graphic file with name nihms-411663-t0007.jpg 43 96
4 4d graphic file with name nihms-411663-t0008.jpg 36 88c
5 4e graphic file with name nihms-411663-t0009.jpg 26 94c
6 4f graphic file with name nihms-411663-t0010.jpg 57 90
7 4g graphic file with name nihms-411663-t0011.jpg 41 94
8 4h graphic file with name nihms-411663-t0012.jpg 32 98
9 4i graphic file with name nihms-411663-t0013.jpg 28 98
10 4j graphic file with name nihms-411663-t0014.jpg 38 94
11 4k graphic file with name nihms-411663-t0015.jpg 47 98
a

Yield (%) for 4a–k in two steps from 11. Dehydrated side products account for the bulk of the balance except for 4d and 4e.

b

The percentage was calculated by integrating HPLC chromatogram peaks at 230 nm.

c

Unidentified oxidized compounds [M + 16] account for the balance.