Table 1.
Data collection and refinement statistics parameters
| Parameter | Value(s) fora: |
|
|---|---|---|
| SSL4 | sLex complex | |
| Crystal data | ||
| Space group | C2 | I222 |
| Cell | ||
| Axial lengths (Å) | 96.1, 81.2, 57.3 | 61.9, 78.9, 97.7 |
| Angles (°) | 90.00, 105.45, 90.00 | 90.00, 90.00, 90.00 |
| Data collection | ||
| Resolution range (Å) | 27.62–1.70 (1.79–1.70) | 24.42–2.50 (2.64–2.5) |
| Data collection temp (K) | 113 | 113 |
| No. of unique reflections | 46,435 | 8,563 |
| Completeness (%) | 99.7 (99.3) | 99.9 (100.00) |
| Mosaicity (°) | 1.02 | 0.214 |
| Rmerge (%) | 0.058 (0.698) | 16.9 (74.7) |
| I/σa | 17.4 (2.4) | 12.0 (3.1) |
| Refinement | ||
| Resolution range (Å) | 27.62–1.70 | 24.42–2.50 |
| R/Rfree | 0.2086/0.2614 | 0.1847/0.2543 |
| Mean B-value (Å2) | 29.7 | 25.6 |
| RMSD from standard values | ||
| Bond lengths (Å) | 0.025 | 0.017 |
| Bond angles (°) | 2.1 | 1.8 |
| Ramachandran plot | ||
| % of residues in favored regions | 97.1 | 95.3 |
| Outliers | None | None |
a
Throughout, values in parentheses are for the outermost resolution shell.