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. 2012 Sep 12;287(45):38178–38189. doi: 10.1074/jbc.M112.376434

TABLE 2.

SAXS data collection and scattering derived parameters for construct EpfNDUF1-3

Data collection parameters
    X-ray source Australian Synchrotron
    Wavelength (Å) 1.127
    q range (Å−1) 0.004–0.25
    Sample flow rate (4 μl s−1) 4
    Exposure time/frame (s) 1
    Concentration range (mg ml−1) 0.25–2.0

Structural parameters
    I(0) (cm−1) (from Guinier plot)
        2 mg ml−1 0.108 ± 0.0001
        1 mg ml−1 0.051 ± 0.0001
        0.5 mg ml−1 0.025 ± 0.0001
        0.25 mg ml−1 0.012 ± 0.0001
    Rg (Å) (from Guinier plot)
        2 mg ml−1 58.2 ± 0.4
        1 mg ml−1 57.6 ± 0.7
        0.5 mg ml−1 56.9 ± 1.2
        0.25 mg ml−1 57.3 ± 1.7
    I(0) (cm−1) (from P(r))a 0.112 ± 0.001
    Rg (Å) (from P(r))a 63.1 ± 0.4
    Dmax (Å)a 215
    Molecular mass Mr (from I(0))a 74,150
    Calculated monomeric mass Mr from sequence 63,184
    Normalized spatial discrepancy of averaged dummy atom modelsa 0.62 ± 0.07

a Reported for 2 mg ml−1 measurement, which was used for model building.