Hardware | Parameter | Start-up setting | Running setting | Resting setting |
8,400 Bruker (Varian) Autosampler | ||||
Injection mode | Spme | Spme | n/a | |
Solvent penetration depth | 0% | 20% | n/a | |
Sample penetration depth | 20% | 20% | n/a | |
Absorption time | 0.01 min | 3 min | n/a | |
Desorption time | 19 min | 1 min | n/a | |
Clean mode solvent source | I | I | n/a | |
Clean mode adsorption and desorption time | 0.01 min | 0.01 min | n/a | |
Water bath (heats autosampler)* | 50 °C | 50 °C | Off | |
CP-3800 Varian Gas Chromatograph | ||||
Injector Oven | Oven power | On | On | On |
Oven temperature | 250 °C | 220 °C | 30 °C | |
Column Oven | Stabilization time | 0.10 min | 0.10 min | 0.10 min |
Temperature | 65 °C | 65 °C | 30 °C | |
Column | Mobile phase flow rate | 8.5 ml/min | 8.5 ml/min | n/a |
Column Pressure | ~ 6 psi | ~ 6 psi | ≥ 0.1 psi | |
FID detector | Oven power | On | On | On |
Temperature | 220 °C | 220 °C | 120 °C | |
Electronics | On | On | Off | |
Time constant | Fast | Fast | Fast | |
Range | 11 | 11 | 11 | |
Autozero | Yes | Yes | Yes |