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. 2012 Sep 5;(67):4142. doi: 10.3791/4142
Hardware Parameter Start-up setting Running setting Resting setting
8,400 Bruker (Varian) Autosampler
Injection mode Spme Spme n/a
Solvent penetration depth 0% 20% n/a
Sample penetration depth 20% 20% n/a
Absorption time 0.01 min 3 min n/a
Desorption time 19 min 1 min n/a
Clean mode solvent source I I n/a
Clean mode adsorption and desorption time 0.01 min 0.01 min n/a
Water bath (heats autosampler)* 50 °C 50 °C Off
CP-3800 Varian Gas Chromatograph
Injector Oven Oven power On On On
Oven temperature 250 °C 220 °C 30 °C
Column Oven Stabilization time 0.10 min 0.10 min 0.10 min
Temperature 65 °C 65 °C 30 °C
Column Mobile phase flow rate 8.5 ml/min 8.5 ml/min n/a
Column Pressure ~ 6 psi ~ 6 psi ≥ 0.1 psi
FID detector Oven power On On On
Temperature 220 °C 220 °C 120 °C
Electronics On On Off
Time constant Fast Fast Fast
Range 11 11 11
Autozero Yes Yes Yes